+ Site Statistics
+ Search Articles
+ PDF Full Text Service
How our service works
Request PDF Full Text
+ Follow Us
Follow on Facebook
Follow on Twitter
Follow on LinkedIn
+ Subscribe to Site Feeds
Most Shared
PDF Full Text
+ Translate
+ Recently Requested

Components detected by means of solid-phase microextraction and gas chromatography/mass spectrometry in the headspace of artisan fresh goat cheese smoked by traditional methods



Components detected by means of solid-phase microextraction and gas chromatography/mass spectrometry in the headspace of artisan fresh goat cheese smoked by traditional methods



Journal of Dairy Science 87(2): 284-299



The study of the headspace components of fresh smoked goat cheese, was carried out by means of solid-phase microextraction using a polyacrylate fiber followed by gas chromatography/mass spectrometry. The samples studied were six artisan Palmero cheeses manufactured following traditional methods and smoked using pine needles. The cheese regions studied were exterior, interior, and a cross section. In total, more than 320 components were detected, the exterior region being the richest in components, among which were acids, alcohols, esters, hydrocarbons, aldehydes, ketones, furan and pyran derivatives, terpenes and sesquiterpenes, nitrogen derivatives, phenol, guaiacol and syringol derivatives, ethers, and others. In addition to typical cheese components, typical smoke components were also detected; these latter were present especially in the headspace of the exterior region and only those in significant concentrations in the exterior region were also detected in the interior. The main components were acids and phenolic derivatives. These latter compounds play an important role in the flavor of this cheese, and their relative proportions together with the presence of specific smoke components derived from pine leaves may be considered of interest in order to distinguish this cheese from others smoked with different vegetable matter.

Please choose payment method:






(PDF emailed within 0-6 h: $19.90)

Accession: 004084513

Download citation: RISBibTeXText

PMID: 14762071

DOI: 10.3168/jds.s0022-0302(04)73167-7


Related references

Components detected by headspace-solid phase microextraction in artisanal fresh goat's cheese smoked using dry prickly pear (Opuntia ficus indica). Lait 84(4): 385-397, 2004

Headspace volatile components of smoked swordfish (Xiphias gladius) and cod (Gadus morhua) detected by means of microextraction and gas chromatography-mass spectrometry. Food chemistry 94(1): 151-156, 2006

Volatile components of raw and smoked black bream and rainbow trout studied by means of solid phase microextraction and gas chromatography/mass spectrometry. Journal of the Science of Food & Agriculture 82(9): 945-952, 2002

Volatile components of raw and smoked black bream (Brama raii) and rainbow trout (Oncorhynchus mykiss) studied by means of solid phase microextraction and gas chromatography/mass spectrometry. Journal of the Science of Food and Agriculture 82(9): 945-952, 2002

Optimization of headspace experimental factors to determine chlorophenols in water by means of headspace solid-phase microextraction and gas chromatography coupled with mass spectrometry and parallel factor analysis. Analytica Chimica Acta 754: 20-30, 2012

Volatile constituents of Murraya koenigii fresh leaves using headspace solid phase microextraction--gas chromatography-mass spectrometry. Natural Product Communications 9(12): 1783-1786, 2014

Gas chromatography-mass spectrometry determination of 3-mercaptohexan-1-ol and 3-mercaptohexyl acetate in wine: a comparison of headspace solid phase microextraction and solid phase extraction methods. Analytica Chimica Acta 596(2): 291-297, 2007

Headspace solid-phase microextraction-gas chromatography-mass spectrometry for analysis of volatile components from pollen pini. Zhong Yao Cai 30(12): 1521-1525, 2007

Headspace solid-phase microextraction-gas chromatography-mass spectrometry for analysis of volatile components from Atractlodes macrocephala Koidz. Se Pu 25(1): 43-47, 2007

Gas chromatography-mass spectrometry following microwave distillation and headspace solid-phase microextraction for fast analysis of essential oil in dry traditional Chinese medicine. Journal of Chromatography. a 1133(1-2): 29-34, 2006

Investigations on the emission of fragrance allergens from scented toys by means of headspace solid-phase microextraction gas chromatography-mass spectrometry. Journal of Chromatography. a 1217(18): 3136-3143, 2010

Application of multiple headspace-solid-phase microextraction followed by gas chromatography-mass spectrometry to quantitative analysis of tomato aroma components. Journal of Chromatography. a 1216(1): 127-133, 2009

Identification and quantification of odorous compounds from adhesives used in food packaging materials by headspace solid phase extraction and headspace solid phase microextraction coupled to gas chromatography-olfactometry-mass spectrometry. Analytica Chimica Acta 745: 53-63, 2012

Analysis of volatile compounds emitted from fresh Syringa oblata flowers in different florescence by headspace solid-phase microextraction-gas chromatography-mass spectrometry. Analytica Chimica Acta 576(1): 43-49, 2006

Rapid determination of paeonol in traditional Chinese medicinal preparations by microwave-assisted extraction followed by headspace solid-phase microextraction and gas chromatography-mass spectrometry. Journal of Analytical Chemistry 66(3): 285-289, 2011