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Development of an analytical method for aminocarb and some derivatives in water using xad resins and gas chromatography


International Journal of Environmental Analytical Chemistry 16(2): 139-148
Development of an analytical method for aminocarb and some derivatives in water using xad resins and gas chromatography
The recovery from water of aminocarb and several of its derivatives using Amberlite XAD resins and the subsequent analysis by GC [gas chromatography] using a N-P detector, was studied. Aminocarb and 3 derivatives, MATACIL phenol, methyl formylamino MATACIL and formylamino MATACIL phenol, were extracted from water at pH 7.0 using Amberlite XAD-4, with > 80% recovery. A 4th derivative, formylamino MATACIL was recovered at .apprx. 70%. The use of other resins such as Amberlite XAD-2 and 7 was more limited although each could be used for the extraction of aminocarb from water. The amphoteric derivative, amino MATACIL phenol, was recovered with XAD-7 but the column had to be eluted with methanol. One derivative, methylamino MATACIL could not be recovered successfully. Experiments with environmental water showed that the % recoveries were good for aminocarb, MATACIL phenol, methyl formylamino MATACIL and formylamino MATACIL.


Accession: 005132332

DOI: 10.1080/03067318308078356



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