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Preparation of methyl 3 dl alanylamido 3 6 dideoxy alpha d gluco pyranoside


, : Preparation of methyl 3 dl alanylamido 3 6 dideoxy alpha d gluco pyranoside. Chemicke Zvesti 38(3): 405-408

The preparation of this compound by the reaction of methyl 3-amino-3,6-dideoxy-.alpha.-D-glucopyranoside with N-benzyloxycarbonyl-D,L-alanine and the subsequent hydrogenolysis of the product is reported. The antibacterial activity of this compound is described.

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Related references

Horner M.W.; Hough L.; Richardson A.C., 1971: Syntheses of methyl 2 4 dibenzamido 2 4 dideoxy alpha d gluco pyranoside and galacto pyranoside. Carbohydrate Research 17(1): 209-212

Jezo I.; Zemek J., 1983: Preparation of methyl 3 6 dideoxy 3 l glyceroylamidoalpha d gluco pyranoside. The preparation of the above compound by the reaction of methyl 3-amino-3,6-dideoxy-.alpha.-D-glucopyranoside with methyl L-glycerate and the antibacterial activity of the obtained product are described.

Pozsgay V.; Neszmelyi A., 1980: Synthesis and carbon 13 nmr spectral study of methyl 2 6 dideoxy alpha l arabino hexo pyranoside methyl 3 6 dideoxy alpha l arabino hexo pyranoside and methyl 4 6 dideoxy alpha l lyxo hexo pyranoside. Carbohydrate Research 85(1): 143-150

Sakakibara T.; Sudoh R., 1983: Reactions of methyl 4 6 o benzylidene 2 3 dideoxy 3 nitro alpha d erythro hex 2 eno pyranoside and methyl 4 6 o benzylidene 2 3 dideoxy 3 nitro beta d erythro hex 2 eno pyranoside with phenyl acetonitrile preparation and structural determination of adducts and an isoxazole derivative. Treatment of methyl 4,6-O-benzylidene-2,3-dideoxy-3-nitro-.alpha.-D-erythro-hex-2-enopyranoside with phenylacetonitrile afforded adducts having the D-manno and D-gluco configurations, the isoxazole 6, the cyano alkene 7, and the nitro alcohols 9 a...

Galemmo R.A.Jr; Horton D., 1983: Preparative routes to methyl 2 acetamido 2 6 dideoxy alpha d gluco pyranoside. Carbohydrate Research 119: 231-240

Evtushenko, E.V.; Ovodov-Yu, S., 1982: Partial methylation of methyl alpha d gluco pyranoside 1. liquid chromatography of acetates of tri o methyl ethers of methyl alpha d gluco pyranoside. A method was described for obtaining acetates of tri-O-methyl ethers of methyl .alpha.-D-glucopyranoside on the basis of partial methylation of methyl .alpha.-D-glucopyranoside. Preparative liquid chromatography was subsequently performed.

Brimacombe J.S.; Doner L.W., 1974: Branched chain sugars part 2 characterization of methyl 2 4 di 3 acetyl 3 6 dideoxy 3 c methyl 3 nitro alpha l gluco pyranoside and some of its chemical transformations. Journal of the Chemical Society Perkin Transactions I (1): 62-65

Haverkamp J.; Van Dongen J.P.C.M.; Vliegenthart J.F.G., 1973: Pmr and carbon 13 magnetic resonance spectroscopy of methyl 2 3 4 6 tetra o methyl alpha d gluco pyranoside and 2 3 4 6 tetra o methyl beta d gluco pyranoside an application to the identification of partially methylated glucoses. Tetrahedron 29(21): 3431-3439

Baer H.H.; Astles D.J., 1984: Preparation of methyl 3 6 dideoxy alpha d xylo hexo pyranoside methyl alpha abequoside and its alpha l lyxo isomer by reduction of epoxides with lithium tri ethyl borohydride. Carbohydrate Research 126(2): 343-347

Evtushenko, E.V.; Ovodov-Yu, S., 1982: Partial methylation of methyl alpha d gluco pyranoside 2. preparative liquid chromatography and gas liquid chromatography of acetates of mono o methyl and di o methyl ethers of methyl alpha d gluco pyranoside. A method was described for preparing and characterizing acetates of mono-and di-O-methyl ethers of methyl .alpha.-D-glucopyranoside. Compounds were isolated by preparative liquid chromatography and GLC of products of partial methylation of methyl...