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Synthesis of lipids and their models on the basis of alkylene phosphites 4. synthesis of phosphatidyl thio phosphatidyl homo cholines and phosphatidyl n n di methyl homo ethanolamines



Synthesis of lipids and their models on the basis of alkylene phosphites 4. synthesis of phosphatidyl thio phosphatidyl homo cholines and phosphatidyl n n di methyl homo ethanolamines



Bioorganicheskaya Khimiya 6(7): 1087-1093



A simple synthetic route is suggested for preparing phosphatidylhomocholines and -N,N-dimethylethanolamines and their thio analogs. The method involves the NaI reaction with easily available 1,2-disubstituted glycerol 1,3-propylenephosphates and thiophosphates followed by aminolysis of intermediate iodopropylphosphates and thiophosphates. A special method was worked out to introduce the fatty acid residues into phosphoglycerides by acylating 1,2-isopropylidine glycerophosphates with fatty acid chlorides.

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