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Synthesis of methyl 3 o 3 6 dideoxy alpha d xylo hexopyranosyl alpha d manno pyranoside



Synthesis of methyl 3 o 3 6 dideoxy alpha d xylo hexopyranosyl alpha d manno pyranoside



Acta Chemica Scandinavica Series B Organic Chemistry and Biochemistry 30(4): 300-304



The synthesis of methyl 3-O-(3,6-dideoxy-.alpha.-D-xylo-hexopyranosyl)-.alpha.-D-mannopyranoside, required for immunological studies of Salmonella, is described. The glycosylation was performed by the Helferich procedure and the influence of a p-nitrobenzoyl group or a non-participating benzyl group in the 2-position in the 3,6-dideoxyhexosyl bromide used was investigated.

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