+ Site Statistics
+ Search Articles
+ PDF Full Text Service
How our service works
Request PDF Full Text
+ Follow Us
Follow on Facebook
Follow on Twitter
Follow on LinkedIn
+ Subscribe to Site Feeds
Most Shared
PDF Full Text
+ Translate
+ Recently Requested

Capillary electrophoretic analysis of salicin in Salix spp

Capillary electrophoretic analysis of salicin in Salix spp

Journal of Chromatography A 781(1-2): 487-490

Salicin is a phenolic glycoside in willow bark which exhibits analgesic effects. Its occurrence in willow (Salix) species is the major reason willow bark and its extracts are popular products in the nutritional supplement market. Previously, HPLC has been the standard method of analysis of quantifying salicin in Salix. We describe a new method of analysis using capillary electrophoresis (CE) that is faster, relatively simple and highly reproducible. Two different species of willow, Salix alba and Salix scouleriana, are analyzed for salicin by CE, using 20 mM glycine (pH 8.8), in uncoated capillaries at 25 kV and 25 degree C, and UV detection at 215 nm.

Please choose payment method:

(PDF emailed within 0-6 h: $19.90)

Accession: 008261736

Download citation: RISBibTeXText

DOI: 10.1016/s0021-9673(97)00492-5

Related references

High-performance liquid chromatographic, capillary electrophoretic and capillary electrophoretic-electrospray ionisation mass spectrometric analysis of selected alkaloid groups. Journal of Chromatography, A 967(1): 85-113, 2002

Isolation of salicin and salireposide from Salix rosmarinifolia L. Acta Poloniae Pharmaceutica 25(6): 591-595, 1968

Extraction of salicin from the bark of Salix humboltiana Willdenow. Rev. Fac. Cienc. quim. La Plata. 16: 171-84, 1941

Salicin derivatives from Salix glandulosa and their biological activities. Fitoterapia 106: 147-152, 2015

Pathways of salicyl alcohol and salicin formation in Salix purpurea L. Phytochemistry 6: 245-52. bibl 22, 1967

The significance of salicin for a Salix-feeder, Phratora (Phyllodecta) vitellinae. Proceedings of the 5th International Symposium on Insect Plant Relationships, Wageningen, the Netherlands, 1-4 March 1982: 73-79, 1982

Isolation of salicin from Salix safsaf F. and a new TLC-colorimetric method for its estimation. Egyptian journal of pharmaceutical sciencesub 1982) 20(1-4): 165-173, 1982

The investigation of the amount of liberated salicin from tablets of Salix Cortex (Labofarm). Herba Polonica 43(2): 145-149, 1997

Validated HPTLC methods for the determination of salicin in Salix sp. and of harpagoside in Harpagophytum [corrected] procumbens. Journal of Pharmaceutical and Biomedical Analysis 48(3): 587-591, 2008

Application of high-performance liquid chromatography for research of salicin in bark of different varieties of Salix. Medicina 45(8): 644-651, 2009

Performance of willow clones on Sharkey clay Salix nigra, Salix exigua, Salix argentinensis, Salix babylonica X Salix alba, interspecific hybrids, selection, Mississippi. US Forest Service research note SO United States Southern Forest Experiment Station: 83 (293), 1983

Chromatographic, capillary electrophoretic and capillary electrochromatographic techniques in the analysis of flavonoids. Journal of Chromatography. A 1073(1-2): 201-227, 2005

Capillary electrophoretic analysis of carbohydrates derivatized by in-capillary condensation with 1-phenyl-3-methyl-5-pyrazolone. Journal of Chromatography. a 911(2): 259-267, 2001