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Solution conformation and dynamics of a tetrasaccharide related to the Lewix(X) antigen deduced by 1H NMR NOESY, ROESY, and T-ROESY measurements


Solution conformation and dynamics of a tetrasaccharide related to the Lewix(X) antigen deduced by 1H NMR NOESY, ROESY, and T-ROESY measurements



Carbohydrate Research 300(1): 3-10



ISSN/ISBN: 0008-6215

PMID: 9203332

DOI: 10.1016/s0008-6215(97)00034-7

The conformational and dynamical features of a Le-X tetrasaccharide analogue GalNAc(alpha-1-3)Gal(beta-1-4)(Fuc(alpha-1-3))Glc(beta-OMe) 1 have been studied through 1H NMR relaxation measurements. The results indicate that the different glycosidic linkages of 1 present distinct conformational flexibility in solution. In addition, the use of T-ROESY experiments in conformational analysis of oligosaccharides is explored emphasizing its scope and limitations.

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Accession: 009432353

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