Section 33
Chapter 32,066

Isolation and recovery of selected polybrominated diphenyl ethers from human serum and sheep serum coupling reversed-phase solid-phase disk extraction and liquid-liquid extraction techniques with a capillary gas chromatographic electron capture negative ion mass spectrometric determinative technique

Loconto,P.R.; Isenga,D.; O'Keefe,M.; Knottnerus,M.

Journal Of Chromatographic Science: 1, 53-60


ISSN/ISBN: 0021-9665
Accession: 032065943

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Polybrominated diphenyl ethers (PBDEs) are isolated and recovered with acceptable percent recoveries from human serum via liquid-liquid extraction and column chromatographic cleanup and fractionation with quantitation using capillary gas chromatography-mass spectrometry with electron capture negative ion and selected ion monitoring. PBDEs are found in unspiked serum.

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