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Fourier transform infrared spectroscopic determination of cypermethrin and deltamethrin in emulsifiable concentrate formulations

Sharma, K.K.; Gupta, S.; Handa, S.K.

Talanta 44(11): 2075-2079

1997


ISSN/ISBN: 0039-9140
PMID: 18966955
DOI: 10.1016/s0039-9140(97)00056-8
Accession: 053292466

Fourier tranform infrared (FT-IR) spectroscopic method has been developed for determination of cypermethrin and deltamethrin in emulsifiable concentrate formulations. The known concentration of formulation was subjected to preparative thin layer chromatography and the active ingradient zone was scrapped from the plate. Pyrethroids were eluted from the adsorbent with chloroform and estimated by measuring the ester carbonyl absorption band at 1749 cm(-1) in cypermethrin and at 1743 cm(-1) in deltamethrin using base line technique. Recoveries of cypermethrin and deltamethrin from commercial and laboratory prepared formulations were 90 to 97% in both the cases. The validity of FT-IR method was confirmed by comparing the results with standard HPLC method.

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