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Sonochemical synthesis and characterization of nano-belt lead(II) coordination polymer: new precursor to produce pure phase nano-sized lead(II) oxide



Sonochemical synthesis and characterization of nano-belt lead(II) coordination polymer: new precursor to produce pure phase nano-sized lead(II) oxide



Ultrasonics Sonochemistry 18(1): 80-84



Nanobelts of new a lead(II) coordination polymer, [Pb(3-pyc)(2)](n) (1), 3-Hpyc=3-pyridinecarboxilic acid were synthesized by a sonochemical method. The new nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The thermal stability of compound was studied by thermal gravimetric and differential thermal analyses. After calcination of nano-sized compound 1 at 400°C, pure phase nano-sized lead(II) oxide has been produced.

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Accession: 055852788

Download citation: RISBibTeXText

PMID: 20580594

DOI: 10.1016/j.ultsonch.2010.01.011


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