Top Buy Now Summary References
Home
>
Section
>
Chapter

Features of Transmission EBSD and its Application

Suzuki, S.

JOM 65(9): 1254-1263

2013

ISSN/ISBN: 1047-4838
DOI: 10.1007/s11837-013-0700-6
Accession: 084010096

Full-Text Article emailed within 0-6 h
Payments are secure & encrypted
Powered by Stripe
Powered by PayPal

Summary
Features of transmission electron backscatter diffraction (EBSD) observation with a standard Ebsd (s-EBSD) detector are surveyed in this study. Heavily deformed Al and 8Cr tempered martensite transmission electron microscope (TEM) specimens were used for this study. It is shown that a specimen tilt angle of ~30°–40° in the opposite direction of the usual 70° and a smaller working distance in the range 4 mm–5 mm are recommended when using a s-Ebsd detector. Specimen thickness and accelerating voltage (Acc. V) have a strong affect on the quality of transmission Ebsd patterns and orientation maps. Higher Acc. Vs are generally recommended to get good quality orientation maps. In case of very thin specimens, lowering the Acc. Vs will give better results. In the observation of a thin film of an 8Cr tempered martensite steel specimen, it is confirmed that t-Ebsd can provide images and detailed quantitative orientation data comparable with that obtained by TEM. It is also shown that small precipitates of Cr23C6 with sizes around 30 nm could be detected and their orientations measured.

References

Ding, R.; Chiu, Y.; Jones, I. P.; Escale, N.; Pettinari-Sturmel, F.; Douin, J. 2012: Application of a novel EBSD-FIB method to the transmission of c + a dislocations through / interfaces Ti-6Al-4V for producing in situ tension transmission electron microscopy specimens Journal of Electron Microscopy 61(1): 31-36
Floer, W.; Hu, Y.M.; Krupp, U.; Christ, H.J. 2002: Application of the EBSD technique to study the initiation and propagation of short cracks - Einsatz der EBSD-Technik zur Untersuchung der Entstehung und Ausbreitung von kurzen Rissen Praktische Metallographie 39(7): 359-368
Avishai, A.; Carter, J.; Zahiri Azar, M.; Narayanan, B.; Heuer, A.H. 2013: Transmission Ebsd - Bridging the Gap between Sem and Tem Microscopy and Microanalysis 19(S2): 694-695
Rice, K.P.; Keller, R.R.; Stoykovich, M.P. 2015: Beam Broadening in Transmission EBSD Microscopy Today 23(2): 32-37
Rice, K.P.; Chen, Y.; Keller, R.R.; Stoykovich, M.P. 2017: Beam broadening in transmission and conventional EBSD Micron 95: 42-50
Rice, K P.; Keller, R R. 2014: Thickness-Dependent Beam Broadening in Transmission EBSD Microscopy and Microanalysis 20(S3): 854-855
Abbasi, M.; Kim, D.-I.; Guim, H.-U.; Jung, W.-S. 2016: Transmission-Ebsd using high Current Electron Beams Microscopy and Microanalysis 22(S3): 1652-1653
Van Bremen, R.; Ribas Gomes, D.; de Jeer, L.T.H.; Ocelík, V.; De Hosson, J.T.M. 2016: On the optimum resolution of transmission-electron backscattered diffraction (t-EBSD) Ultramicroscopy 160: 256-264
Duber, O.; Kunkler, B.; Krupp, U.; Christ, H.J.; Fritzen, C.P. 2006: Gefügecharakterisierung mehrphasiger Werkstoffe mittels EBSD - Characterizing the microstructure of multiphase materials using EBSD Praktische Metallographie 43(2): 88-102
Heimann, S.; Knyazeva, M.; Pohl, M. 2010: EBSD-Gefügeuntersuchungen an Aluminiummatrix-Verbundwerkstoffen - EBSD-Microstructural Investigations on Aluminium Matrix Composite Materials Praktische Metallographie 47(11): 640-653
McCabe, R; Proust, G; Misra, A; Cerreta, E; Henrie, B 2006: EBSD and Coupled EBSD/TEM Analysis of Zirconium Deformation Mechanisms Microscopy and Microanalysis 12: 1024-0
Zaefferer, S.; Konijnenberg, P. 2012: Advanced analysis of 3D EBSD data obtained from FIB-EBSD tomography Microscopy and Microanalysis 18(S2): 520-521
Cotrina, E.; Izamendia, A.; Lopez, B.; Gutierrez, I. 2004: AplicaciÓn de las técnicas de EBSD al estudio de la transformaciÓn γ-α en aceros microaleados - Study of the γ-α transformation in microalloyed steels by EBSD techniques Revista de Metalurgia (Madrid) 40(5): 359-364
Koblischka-Veneva, A.; Koblischka, M.R.; Schmauch, J.; Noudem, J.; Murakami, M. 2019: Analysis of the microstructure of bulk MgB2 using TEM, EBSD and t-EBSD Journal of Microscopy 274(3): 123-131
Sitzman, S. 2018: Tutorial: Ultra-high Spatial Resolution Ebsd: Transmission Kikuchi Diffraction (Tkd) in the Sem Microscopy and Microanalysis 24(S1): 2324-2325
Altuna, M.A.; Gutierrez, I. 2008: Aplicación de técnicas de nanoindentación y EBSD en aceros con microestructuras complejas - Aplication of nanoindentation and EBSD techniques in complex microstructures steels Revista de Metalurgia (Madrid) 44(1): 19-28
Geiss, R; Keller, R; Read, D 2010: Transmission Electron Diffraction From Nanoparticles, Nanowires and Thin Films in an SEM With Conventional EBSD Equipment Microscopy and Microanalysis 16: 1742-1743
Wang, J.; Huang, M.; Hu, J.; Wang, C.; Xu, W. 2021: EBSD investigation of the crystallographic features of deformation-induced martensite in stainless steel Journal of Materials Science-Technology 69: 148-155
Novillo, E.; Petite, M.M.; Bocos, J.L.; Gutierrez, I. 2004: Análisis mediante EBSD de los procesos de recristalizaciÓn y crecimiento de grano en un acero ULC - Analysis of recrystallization and grain growth in ultra low carbon steels using EBSD Revista de Metalurgia (Madrid) 40(5): 352-358
Kral, M.V.; Drabble, D.J.F.; Gardiner, B.R.; Tait, P.C. 2009: Implications of EBSD-based Grain Size Measurement on Structure-Property Correlations - Auswirkungen der Korngrössenmessung mit der EBSD auf die Wechselbeziehungen zwischen Struktur und Eigenschaften Praktische Metallographie 46(9): 469-482